Finishing up on the IEEE 3DIC meeting from Oct 2013 in San Francisco lets look at some of the remaining key papers from the conference.
Tohoku Univ - Lattice Distortions in Thinned Silicon
Professor Koyanagi and coworkers at Tohoku Univ and GINTI [ Global Integration Initiative – see IFTLE 166, “IEEE 3DIC Conf part 1; 3DIC panel discussion; Ginti; Novati” ]
It is accepted that to achieve compact-sized 3DIC each functional wafer should be thinned to 50μm or less. However, the ultra-thin nature of Si substrate leads to several problems such as weak mechanical strength, warping and local deformation in the stacked die . Moreover, the weak mechanical strength of the extremely thin die/wafer itself has a potential concern lead to die breaking for 3DIC integration, because thin LSI chip with high density TSVs is highly fragile and more easily damaged. Hence, it is important to understand the impact of chip’s mechanical strength on device reliabilities decreasing die thickness, especially below 50μm thickness.
Koyonagi and co-workers have found that the Young`s modulus (E) of Si substrate begins to noticeably decrease below 50μm thickness. The Young`s modulus in 30μm thick Si is 30% of the modulus of 50μm thickness. In 30μm Si the lattice structure is highly distorted which induces the Young`s modulus reduction and consequently weakens the mechanical strength.
DRAM chip of 200μm thickness were bonded to a Si interposer and thinned down to 50, 40, 30 and 20μm respectively. The measured retention characteristics of DRAM cell on these thicknesses of silicon are degraded dramatically below 50-μm thickness, i.e. the retention time of DRAM cell in 20μm thick chip is shortened by approximately 40% compared to the 50-μm thick chip.
They assume that the band-gap energy in the thin chip is affected by the distortion of the lattice structure, hence effect on a minority carrier lifetime, consequently shortening the retention time of DRAM cell.
Fujitsu – Influence of Wafer Thinning on Backside Damage
Fujitsu is known for their ultrathin WOW process [ see “Development of Multistack Process on Wafer-on-Wafer (WOW)”
Ultra-thinning to 10 microns or less of Si wafer is expected to realize small TSV with low aspect ratio and coupling capacitance. Subsurface damage following wafer thinning from the back of 300 mm wafers using three different types of thinning process was investigated by means of Raman spectroscopy, XTEM, and Positron annihilation analysis, respectively. A coarse grinding generates significant rough subsurface ranged several micron and damage layer including amorphous and plastic-deformed Si along grinding topography. Fine grinding, second step of thinning, reduced those surface roughness and almost removed after thinning at least removal of 50 microns. However, plastic-deformed subsurface layer with a thickness of 100 to 200 nm are still remained which leaves an inside elastic stress layer ranging up to about 10 microns in depth. Chemical-Mechanical Polishing (CMP) process as a final step of thinning enables to remove residual damages such as structural defects and lattice strains after 1-5 microns thick polishing while vacancy-type defects only remain.
The authors acknowledge that further investigations are necessary to find “hidden residual defects” and to understand the influence of thinning on memory devices (see Tohoku discussions above).
ASE / Chiao Tung Univ – Low Temp Bonding
ASE and National Chiao Tung Univ have studied three types of bonding, including Cu-In, Sn/In-Cu, and Cu/Ti-Ti/Cu, for application of 3D interconnects.
Cu-In bonding and Sn/In-Cu bonding can form intermetallic compounds at the bonding temperature lower than 180 C. Cu and In samples were bonded face-to-face with a bonding pressure of 1.91 MPa, followed by a heating temperature of 170 C for 50 min. Sn/In and Cu samples were bonded face-to-face with a bonding pressure of 1.91 MPa, at bonding temperature of 180 C for 50 min.
Cu/Ti samples were bonded face to face with a bonding pressure of 1.91 MPa, at a heating temperature of 180 C for 50 min. They add that Cu can be protected from oxidation by capping Ti on Cu surface before bonding. This last structure is especially significant if one can really do such bonding at 180 C . Their EDX investigation of the interface shows that “…apparently there is a Cu layer at the bonding interface instead of Ti layers…due to lower activation energy at the surface, Cu tends to diffuse towards the surface …” IFTLE feels this combination certainly deserves further study.
All bonded structures have shown excellent electrical performance and reliability characteristics. Based on bond results, these structures can be applied for low temperature bonding in 3D interconnects.
RTI – 10um Pitch Bonding of Hetero Materials
Matt Lueck of RTI Int described their successful demonstration of the use and reliability of Cu/Sn microbumps for the fine pitch interconnection of heterogeneous semiconductor die. InP die have been bonded to Si substrates using a 6.4 mm × 5.12 mm area array of alloyed Cu/Sn microbumps on 10 μm pitch.
A key technological challenge facing the 3D integration of heterogeneous semiconductors is the formation of high density metal interconnects between dissimilar substrates, such as compound semiconductors (CS) and Si. Due to the difference in the coefficients of thermal expansion (CTE), one can expect: 1) some misalignment between microbumps fabricated on the CS substrate and the Si substrate during bonding at an elevated temperature; and 2) bond interconnects will experience shear strain as the bonded die pair is cooled to room temperature and during any subsequent thermal excursions.
To estimate the magnitude of the misalignment, they calculated the relative change in distance between corner microbumps in a 10 μm pitch 640 × 512 array on CS die vs. Si die. Operability was determined by electrical testing of long daisy-chains of bumps.
The average channel yield was approximately 97% for both InP-Si and Si-Si die pairs translating into the array operability greater than 99.99%. The reliability of InP-Si and SI-Si die pairs was compared after 500 thermal cycles of -40 – 125 C. No significant change in yield was seen for the homogeneous Si-Si die pairs. The InP-Si die pairs that were underfilled showed a 2.8% decrease in channel yield whereas those not underfilled showed a 13.9% decrease.
They conclude that Cu/Sn micro bumps can be successfully and reliably used for integration of InP and Si die.
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